Hostname: page-component-cd9895bd7-8ctnn Total loading time: 0 Render date: 2024-12-26T09:11:11.305Z Has data issue: false hasContentIssue false
  • English
  • Français

Crystal data of the low-temperature solid form of 2-methyl-2-nitro-propanol(MNP)

Published online by Cambridge University Press:  10 January 2013

J. Ll. Tamarit ,
N. B. Chanh ,
P. Négrier ,
D. O. López ,
M. Barrio  and
Y. Haget
J. Ll. Tamarit
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
N. B. Chanh
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
P. Négrier
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
D. O. López
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
M. Barrio
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
Y. Haget
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
Get access Rights & Permissions [Opens in a new window]

Abstract

By means of X-ray single crystal Weissenberg photographs, the crystal of the low-temperature solid form of 2-methyl-2-nitro-propanol, (CH3)2C(NO2)(CH2OH), has been determined and found to be of the monoclinic type, space group P21/c. The cell constants were refined from X-ray powder diffraction data: a=6.195(3) Å, b=19.116(7) Å, c=16.598(7) Å, and β = 90.12(2)° with Z = 12. The indexed pattern at 293 K is given.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 2 , June 1994 , pp. 84 - 86
Copyright
Copyright © Cambridge University Press 1994

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

AFMAIL, program (1968) (Laboratoire de Cristallographie et Physique Cristalline, Bordeaux).Google Scholar
Barrio, M. (1993). Doctoral thesis. Barcelona.Google Scholar
Boultif, A., and Louer, D. (1991). J. Appl. Cryst. 24, 987–993CrossRefGoogle Scholar
De Wolff, P. M. (1968). J. Appl. Cryst. 5, 108–113.CrossRefGoogle Scholar
Marr, H. E. III, Kruger, G. J., and Stewart, J. M. (1977). Acta Cryst. B 33, 2886–2887.CrossRefGoogle Scholar
Louer, D., and Louer, M. (1972). J. Appl. Cryst. 5, 271–275.CrossRefGoogle Scholar
Louer, D., and Vargas, R. (1982). J. Appl. Cryst. 15, 542–545.CrossRefGoogle Scholar
Sake Gowda, D. S., and Rudman, R. (1982). J. Chem. Phys. 77(9), 4671–4677.CrossRefGoogle Scholar
Smith, G. S., and Snyder, R. L. (1979). J. Appl. Cryst. 12, 60–65.CrossRefGoogle Scholar
Tamarit, J. Ll., Legendre, B. and Buisine, J. M. submitted to Physica B.Google Scholar
Urban, Z.Tomkowicz, ; Mayer, J., and Waluga, T. (1975). Acta Phys. Pol A 48, 61–67.Google Scholar