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Powder X-ray diffraction of 5-Chloro-N-(4-nitrophenyl) pentanamide, C11H13ClN2O3

Published online by Cambridge University Press:  13 August 2015

Qing Wang ,
Yan Mei Huang ,
Qiao Mei Sun ,
Xiang Ling Ma  and
Hui Li
Qing Wang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Yan Mei Huang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Qiao Mei Sun
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Xiang Ling Ma
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com
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Abstract

X-ray powder diffraction data for 5-Chloro-N-(4-nitrophenyl)pentanamide, C11H13ClN2O3, are reported [a = 8.036(4) Å, b = 15.972(5) Å, c = 9.829(5) Å, α = 90°, β = 104.227(2)°, γ = 90°, V = 1222.98 Å3, Z = 4, ρx = 1.3941 g cm−3 and space group P21/c]. All measured lines were indexed and are consistent with the P21/c space group. No detectable impurities were observed.

Keywords

5-Chloro-N-(4-nitrophenyl) pentanamidepharmaceutical intermediateanticoagulantapixaban
Type
Rapid Communication
Information
Powder Diffraction , Volume 30 , Issue 4 , December 2015 , pp. 365
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Copyright
Copyright © International Centre for Diffraction Data 2015 

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References

Jiang, J. and Ji, Y. (2013). “Alternate synthesis of apixaban (BMS-562247), an inhibitor of blood coagulation factor Xa,” Synth. Commun. 43(1), 72–79.CrossRefGoogle Scholar
Neumann, M. A. (2003). “X-Cell: a novel indexing algorithm for routine tasks and difficult cases,” J. Appl. Crystallogr. 36, 356–365.CrossRefGoogle Scholar
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