Hostname: page-component-78c5997874-dh8gc Total loading time: 0 Render date: 2024-11-13T17:15:56.559Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray Powder Data for Sodium tri-aqua-hexa-(nicotinato-tri-μ-oxo- tri-chromium (III) perchlorate) hexahydrate {Na [Cr3O(C6H5NO2)6 (H2O)3] [ClO4]8·C6H5NO2·6H2O}

Published online by Cambridge University Press:  10 January 2013

D. F. Mullica ,
E. L. Sappenfield  and
J. E. Bradshaw
D. F. Mullica
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
E. L. Sappenfield
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
J. E. Bradshaw
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
Get access Rights & Permissions [Opens in a new window]

Abstract

The indexed X-ray diffraction powder data of sodium triaqua-hexa-(nicotinato-tri-μ-oxo-tri-chromium(III) perchlorate) hexahydrate {Na [Cr3 O(C6H5NO2)6(H2 O)3] [ClO4]8·C6H5NO2·6H2O, NICCR} is reported. NICCR crystallizes in the hexagonal space group P63/m. The refined cell parameters were determined by employing a Siemens Debye-Scherrer camera (Fe Kā radiation, λmean= 1.93736 Å). The cell constants are a = 13.573(2), c = 24.901(5) Å, V = 3972.8 Å3 and Dx =1.68 Mg m-3 (Dm =1.67 Mg m-3). The quantitative figure of merit (FN) for NICCR is F27 = 32(0.010,81). The JCPDS Diffraction File No. is 36–1978.

Type
Research Article
Information
Powder Diffraction , Volume 1 , Issue 3 , September 1986 , pp. 261 - 262
Copyright
Copyright © Cambridge University Press 1986

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Earnshaw, A., Figgis, B. N. and Lewis, J. (1966). J. Chem. Soc.(A), 12, 1656–1663.Google Scholar
Gonzalez-Vergara, E., Hegenauer, J., Saltman, P., Sabat, M. and Ibers, J. A. (1982). Inorg. Chim. Acta, 66, 115–18.CrossRefGoogle Scholar
Mertz, W., Toepfer, E. W., Roginski, E. E., and Polansky, M. M. (1974). Fed. Proc., 33, 2275–2280.Google Scholar
Roof, R. B. Jr., (1968). LASL Report, Los Alamos Scientific Laboratory.Google Scholar
Schenk, K., and Gudel, H. (1982). Inorg. Chem., 21, 2253–2256.Google Scholar
Schwarz, K. and Mertz, W. (1959). Arch. Biochem. Biophys., 85, 292–295.CrossRefGoogle Scholar
Smith, G. S. and Snyder, R. L. (1979). J. Appl. Cryst., 12, 60–65.Google Scholar
Weinland, R. (1908). Ber. dt. Chem. Ges., 41, 3236–3245.CrossRefGoogle Scholar