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X-ray powder diffraction data for tectoridin, C22H22O11

Published online by Cambridge University Press:  02 November 2015

YuanZhi Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
PeiXiao Tang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
KaiLin Xu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
ShanShan Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
LiuQi Guo
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for tectoridin, C22H22O11, are reported [a = 13.577 (2) Å, b = 10.466 (8) Å, c = 9.454 (7) Å, α = 85.709 (4)°, β = 94.855 (3)°, γ = 101.485 (3)°, unit-cell volume V = 1309.50 Å3, Z = 2, ρ = 1.179 × 103 kg m−3, and space group P1]. No detectable impurity was observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2015 

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References

Harris, K. D. M. (2012). “Powder diffraction crystallography of molecular solids,” Top. Curr. Chem. 315, 133178.CrossRefGoogle ScholarPubMed
Lee, Y. S., Kim, S. H., Kim, J. K., Lee, S., Jung, S. H., and Lim, S. S. (2011). “Preparative isolation and purification of seven isoflavones from Belamcanda chinensis ,” Phytochem. Anal. 22(5), 468473.CrossRefGoogle ScholarPubMed
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: powder X-ray diffraction versus single-crystal X-ray diffraction,” Chin. Sci. Bull. 57(30), 38673871.Google Scholar
Qu, J., Gao, J., Sun, J., Zhang, L., Makino, T., and Yuan, D. (2012). “Pharmacokinetics of conjugated metabolites in rat plasma after oral administration of tectoridin,” J. Chromatogr. B 902, 6169.Google Scholar
Tang, P. X., Wu, X. Q., Pan, Q. Q., Zhang, L. L., Cheng, Q., and Li, H. (2013). “X-ray powder diffraction data for norandrostenedione,” Powder Diffr. 28(4), 302304.Google Scholar
Wu, X. Q., Tang, P. X., Pan, Q. Q., Cheng, Q., and Li, H. (2013). “crystal structure determination of three polycyclic compounds and comparative Rietveld refinement between MS and GSAS programs,” Chin. Sci. Bull. 58(20), 24302434.Google Scholar
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