Hostname: page-component-cd9895bd7-jn8rn Total loading time: 0 Render date: 2024-12-26T08:40:47.518Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction pattern for glucopyranosylsorbitol and glucopyranosylmannitol dihydrate

Published online by Cambridge University Press:  10 January 2013

P. Perkkalainen ,
H. Halttunen ,
H. Heikkilä ,
I. Pitkänen  and
J. Valkonen
P. Perkkalainen
Affiliation:
Department of Chemistry, University of Jyväskylä, P.O. Box 35, SF-40351 Jyväskylä, Finland
H. Halttunen
Affiliation:
Department of Chemistry, University of Jyväskylä, P.O. Box 35, SF-40351 Jyväskylä, Finland
H. Heikkilä
Affiliation:
Technology Center, Cultor Ltd., SF-02460 Kantvik, Finland
I. Pitkänen
Affiliation:
Department of Chemistry, University of Jyväskylä, P.O. Box 35, SF-40351, Jyväskylä, Finland
J. Valkonen
Affiliation:
Department of Chemistry, University of Jyväskylä, P.O. Box 35, SF-40351, Jyväskylä, Finland
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder data are given for glucopyranosylsorbitol, C12H24O11, and glucopyranosylmannitol dihydrate, C12H24O11 * 2H2O. Refined unit cell parameters for glucopyranosylsorbitol are: a=0.9124(4) nm, b=1.1336(5) nm, c=0.7232(3) nm, and β=91.23(4)° in space group P21 and those for glucopyranosylmannitol dihydrate are a=2.2579(15) nm, b=1.0016(5) nm, and c=0.7584(5) nm in space group P212121.

Type
Research Article
Information
Powder Diffraction , Volume 12 , Issue 2 , June 1997 , pp. 93 - 95
Copyright
Copyright © Cambridge University Press 1997

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

de Wolff, P. M. (1968). “A Simplified Criterion for Reliability of Powder Pattern Indexing,” J. Appl. Crystallogr. 1, 108–113.CrossRefGoogle Scholar
Dinnebier, R. E., and Pennartz, P. U. (1993). “ENRAF-GUFI, ein Programmpaket zur Messung und Auswertung von Pulveraufnahmen mit dem 120° 2θ ortsempfindlichen Detektor,” Z. Kristallogr., Suppl. 7, 33–34.Google Scholar
Hess, J. B. (1951). “A Modification of the Cohen Procedure for Computing Precision Lattice Constants from Powder Data,” Acta Crystallogr. 4, 209–215.CrossRefGoogle Scholar
Lichtenthaler, H. J., and Lindner, F. W. (1981). “The Preferred Conformations of Glycosylalditols,” Liebigs Ann. Chem. 2372–2383.Google Scholar
Lindner, F. W., and Lichtenthaler, F. W. (1981). “Extended Zigzag Conformation of 1-O-D-α-glucopyranosyl-D-mannitol,” Carbohydr. Res. 93, 135–140.Google Scholar
Schiweck, H., Munir, M., Rapp, K. M., Schneider, B., and Vogel, M. (1990). “New Developments in the Use of Sucrose as an Industrial Bulk Chemical,” Zuckerind astrie 115, 555–565.Google Scholar
Smith, G. S., and Snyder, R. L. (1979). “F N: A Criterion for Rating Powder Diffraction Patterns and Evaluating the Reliability of Powder-Pattern Indexing,” J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar
Werner, P. E. (1969). “A FORTRAN program for least-squares refinement of crystal structure cell dimensions,” Ark. Kemi 31, 513–516.Google Scholar