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14C GIRI SAMPLES IN AMS GOLDEN VALLEY: GRAPHITE PREPARATION USING AGE-3 AND ABSORPTION-CATALYTIC SETUP

Published online by Cambridge University Press:  29 April 2024

E V Parkhomchuk Open the ORCID record for E V Parkhomchuk [Opens in a new window] ,
A V Petrozhitskiy Open the ORCID record for A V Petrozhitskiy [Opens in a new window] ,
M M Ignatov ,
D V Kuleshov ,
A I Lysikov ,
A G Okunev ,
K A Babina  and
V V Parkhomchuk
E V Parkhomchuk*
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia Institute of Archaeology and Ethnography SB RAS, 17 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia Boreskov Institute of Catalysis SB RAS, 5 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
A V Petrozhitskiy
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia Budker Institute of Nuclear Physics Siberian Branch Russian Academy of Sciences (BINP SB RAS), 11 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia Institute of Archaeology and Ethnography SB RAS, 17 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
M M Ignatov
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia Institute of Archaeology and Ethnography SB RAS, 17 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
D V Kuleshov
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia Institute of Archaeology and Ethnography SB RAS, 17 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
A I Lysikov
Affiliation:
Boreskov Institute of Catalysis SB RAS, 5 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
A G Okunev
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia
K A Babina
Affiliation:
Institute of Archaeology and Ethnography SB RAS, 17 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia Boreskov Institute of Catalysis SB RAS, 5 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
V V Parkhomchuk
Affiliation:
Novosibirsk State University, AMS Golden Valley, 2 Pirogova str., Novosibirsk, 630090, Russia Budker Institute of Nuclear Physics Siberian Branch Russian Academy of Sciences (BINP SB RAS), 11 Acad. Lavrentiev Ave., Novosibirsk, 630090, Russia
*
*Corresponding author. Email: ekaterina@catalysis.ru
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Abstract

The AMS Golden Valley laboratory is equipped with two accelerator mass spectrometers: the AMS facility from the Budker Institute of Nuclear Physics (BINP) and the Mini Carbon Dating System (MICADAS-28) from Ionplus AG and two graphitization systems: the Automated Graphitization Equipment (AGE-3) from Ionplus AG and the Absorption-catalytic setup (ACS) developed at the Boreskov Institute of Catalysis (BIC). The ACS was designed for graphite preparation from labeled biomedical samples, dissolved organics, and dissolved or gaseous carbon dioxide but has proven to be suitable for the traditional dating of objects no older than 35,000 years. Here we present two series of AMS data for the samples from Glasgow International Radiocarbon Inter-comparison (GIRI), prepared using AGE-3 and ACS, and then measured on MICADAS-28. The mean value of the background F14C was 0.0024 ± 0.0009 and 0.012 ± 0.003 for AGE-3 and ACS, respectively, and both methods gave reproducible results for the OXI.

Keywords

AMSgraphitization systemsintercomparisonradiocarbon
Type
Conference Paper
Information
Radiocarbon , Volume 66 , Issue 5: 24th Radiocarbon and 10th 14C & Archaeology, Zurich, Sept. 11–16, 2022 Proceedings Part 1 of 2 , October 2024 , pp. 1259 - 1269
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Copyright
© The Author(s), 2024. Published by Cambridge University Press on behalf of University of Arizona

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Footnotes

Selected Papers from the 24th Radiocarbon and 10th Radiocarbon & Archaeology International Conferences, Zurich, Switzerland, 11–16 Sept. 2022.

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