Skip to main content Accessibility help

We use cookies to distinguish you from other users and to provide you with a better experience on our websites. Close this message to accept cookies or find out how to manage your cookie settings.

Close cookie message
×
Hostname: page-component-5b777bbd6c-6lqsf Total loading time: 0 Render date: 2025-06-19T18:19:32.709Z Has data issue: false hasContentIssue false

7 - Electron Beam Effects in Liquid Cell TEM and STEM

from Part I - Technique

Published online by Cambridge University Press:  22 December 2016

By
Nicholas M. Schneider
Edited by
Frances M. Ross
Frances M. Ross
Affiliation:
IBM T. J. Watson Research Center, New York
Get access

Summary

A summary is not available for this content so a preview has been provided. Please use the Get access link above for information on how to access this content.
Image of the first page of this content. For PDF version, please use the ‘Save PDF’ preceeding this image.'
Type
Chapter
Information
Liquid Cell Electron Microscopy , pp. 140 - 163
Publisher: Cambridge University Press
Print publication year: 2016

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Book purchase

Temporarily unavailable

References

Grogan, J. M., Schneider, N. M., Ross, F. M. and Bau, H. H., Bubble and pattern formation in liquid induced by an electron beam. Nano Lett., 14 (2014), 359–364.CrossRefGoogle ScholarPubMed
Schneider, N. M., Norton, M. M., Mendel, B. J. et al., Electron–water interactions and implications for liquid cell electron microscopy. J. Phys. Chem. C, 118 (2014), 22373–22382.CrossRefGoogle Scholar
Spinks, J. W. T. and Woods, R. J., An Introduction to Radiation Chemistry (New York: Wiley-Interscience, 1990).Google Scholar
Allen, A. O., The Radiation Chemistry of Water and Aqueous Solutions (Princeton, NJ: Van Nostrand, 1961).Google Scholar
Draganic, I., The Radiation Chemistry of Water (New York: Elsevier, 2012).Google Scholar
Pastina, B. and LaVerne, J. A., Effect of molecular hydrogen on hydrogen peroxide in water radiolysis. J. Phys. Chem. A, 105 (2001), 9316–9322.CrossRefGoogle Scholar
Elliot, A. J. and McCracken, D. R., Computer modeling of the radiolysis in an aqueous lithium salt blanket: suppression of radiolysis by addition of hydrogen. Fusion Eng. Des., 13 (1990), 21–27.CrossRefGoogle Scholar
Joseph, J. M., Choi, B. S., Yakabuskie, P. and Wren, J. C., A combined experimental and model analysis on the effect of pH and O2(aq) on γ-radiolytically produced H2 and H2O2. Radiation Phys. Chem., 77 (2008), 1009–1020.CrossRefGoogle Scholar
Carron, N. J., An Introduction to the Passage of Energetic Particles through Matter (Boca Raton, FL: CRC Press, 2006).CrossRefGoogle Scholar
Bethe, H. A. and Ashkin, J., Bethe: Passage of radiations through matter. In Segre, E., ed., Experimental Nuclear Physics Vol. 1, (New York: Wiley, 1953).Google Scholar
Berger, M. J., Coursey, J. S., Zucker, M. A. and Chang, J., NIST Stopping-Power and Range Tables: Electrons, Protons, Helium Ions. Available at http://physics.nist.gov/PhysRefData/Star/Text/ESTAR.html [Accessed: 3 November 2014].Google Scholar
LaVerne, J. A. and Pimblott, S. M., Electron energy-loss distributions in solid, dry DNA. Rad. Res., 141 (1995), 208–215.CrossRefGoogle ScholarPubMed
Tabata, T., A simple calculation for mean projected range of fast electrons. J. Appl. Phys., 39 (1968), 5342–5343.CrossRefGoogle Scholar
Rose, M. E., Electron path lengths in multiple scattering. Phys. Rev., 58 (1940), 90.CrossRefGoogle Scholar
Drouin, D., Couture, A. R., Joly, D. et al., CASINO V2.42: a fast and easy-to-use modeling tool for scanning electron microscopy and microanalysis users. Scanning, 29 (2007), 92–101.CrossRefGoogle ScholarPubMed
Zheng, H., Claridge, S. A., Minor, A. M., Alivisatos, A. P. and Dahmen, U., Nanocrystal diffusion in a liquid thin film observed by in situ transmission electron microscopy. Nano Lett., 9 (2009), 2460–2465.CrossRefGoogle Scholar
Schwarz, H. A., Applications of the spur diffusion model to the radiation chemistry of aqueous solutions. J. Phys. Chem., 73 (1969), 1928–1937.CrossRefGoogle Scholar
Buxton, G. V., Greenstock, C. L., Helman, W. P. and Ross, A. B., Critical-review of rate constants for reactions of hydrated electrons, hydrogen-atoms and hydroxyl radicals in aqueous solution. J. Phys. Chem. Ref. Data, 17 (1988), 513–886.CrossRefGoogle Scholar
Hill, M. A. and Smith, F. A., Calculation of initial and primary yields in the radiolysis of water. Rad. Phys. Chem., 43 (1994), 265–280.CrossRefGoogle Scholar
Pimblott, S. M. and LaVerne, J. A., Molecular product formation in the electron radiolysis of water. Rad. Res., 129 (1992), 265–271.CrossRefGoogle ScholarPubMed
Christensen, H., Remodeling of the oxidant species during radiolysis of high-temperature water in a pressurized water reactor. Nucl. Technol., 109 (1995), 373–382.CrossRefGoogle Scholar
Burton, M., Radiation chemistry. J. Phys. Chem., 51 (1947), 611–625.CrossRefGoogle ScholarPubMed
Speight, J., Lange’s Handbook of Chemistry (New York: McGraw-Hill Professional, 2004).Google Scholar
Schneider, N. M./Radiolysis, github.com. Available at https://github.com/NMSchneider/Radiolysis [Accessed: 30 June 2014].Google Scholar
Hart, E. J., The hydrated electron: properties and reactions of this most reactive and elementary of aqueous negative ions are discussed. Science, 146 (1964), 19–25.CrossRefGoogle ScholarPubMed
Grogan, J. M., Rotkina, L. and Bau, H. H., In situ liquid-cell electron microscopy of colloid aggregation and growth dynamics. Phys. Rev. E, 83 (2011), 061405.CrossRefGoogle ScholarPubMed
Mirsaidov, U., Ohl, C.-D. and Matsudaira, P., A direct observation of nanometer-size void dynamics in an ultra-thin water film. Soft Matter, 8 (2012), 7108–7111.CrossRefGoogle Scholar
Huang, T.-W., Liu, S.-Y., Chuang, Y.-J. et al., Dynamics of hydrogen nanobubbles in KLH protein solution studied with in situ wet-TEM. Soft Matter, 9 (2013), 8856–8861.CrossRefGoogle Scholar
Klein, K. L., Anderson, I. M. and de Jonge, N., Transmission electron microscopy with a liquid flow cell. J. Microsc., 242 (2011), 117–123.CrossRefGoogle ScholarPubMed
Jones, S., Bubble nucleation from gas cavities: a review. Adv. Coll. Interf. Sci., 80 (1999), 27–50.CrossRefGoogle Scholar
Li, D., Nielsen, M. H., Lee, J. R. I. et al., Direction-specific interactions control crystal growth by oriented attachment. Science, 336 (2012), 1014–1018.CrossRefGoogle ScholarPubMed
Woehl, T. J., Evans, J. E., Arslan, I., Ristenpart, W. D. and Browning, N. D., Direct in situ determination of the mechanisms controlling nanoparticle nucleation and growth. ACS Nano, 6 (2012), 8599–8610.CrossRefGoogle ScholarPubMed
Noh, K. W., Liu, Y., Sun, L. and Dillon, S. J., Challenges associated with in-situ TEM in environmental systems: the case of silver in aqueous solutions. Ultramicroscopy, 116 (2012), 34–38.CrossRefGoogle Scholar
Lee, J., Urban, A., Li, X. et al., Unlocking the potential of cation-disordered oxides for rechargeable lithium batteries. Science, 343 (2014), 519–522.CrossRefGoogle ScholarPubMed
Bresin, M., Nadimpally, B. R., Nehru, N., Singh, V. P. and Hastings, J. T., Site-specific growth of CdS nanostructures. Nanotechnology, 24 (2013), 505305.CrossRefGoogle ScholarPubMed
Park, J., Kodambaka, S., Ross, F. M., Grogan, J. M. and Bau, H. H., In situ liquid cell transmission electron microscopic observation of electron beam induced Au crystal growth in a solution. Microsc. Microanal., 18 (2012), 1098–1099.CrossRefGoogle Scholar
den Heijer, M., Shao, I., Radisic, A., Reuter, M. C. and Ross, F. M., Patterned electrochemical deposition of copper using an electron beam. APL Materials, 2 (2014), 022101.CrossRefGoogle Scholar
Remita, H., Lampre, I., Mostafavi, M., Balanzat, E. and Bouffard, S., Comparative study of metal clusters induced in aqueous solutions by γ-rays, electron or C6+ ion beam irradiation. Rad. Phys. Chem., 72 (2005), 575–586.CrossRefGoogle Scholar
Abidi, W. and Remita, H., Gold based nanoparticles generated by radiolytic and photolytic methods. Recent Patents in Eng., 4 (2010), 170–188.CrossRefGoogle Scholar
Mullins, W. W. and Sekerka, R. F., Stability of a planar interface during solidification of a dilute binary alloy. J. Appl. Phys., 35 (1964), 444–451.CrossRefGoogle Scholar
Evans, J. E., Jungjohann, K. L., Browning, N. D. and Arslan, I., Controlled growth of nanoparticles from solution with in situ liquid transmission electron microscopy. Nano Lett., 11 (2011), 2809–2813.CrossRefGoogle ScholarPubMed
Zheng, H., Smith, R. K., Jun, Y. W. et al., Observation of single colloidal platinum nanocrystal growth trajectories. Science, 324 (2009), 1309–1312.CrossRefGoogle ScholarPubMed
Mallard, W. G., Ross, A. B. and Helman, W. P., NDRL/NIST Solution Kinetics Database on the Web: A complication of kinetics data on solution-phase reactions. Available at http://kinetics.nist.gov/solution/ [Accessed: 6 April 2015].Google Scholar
Park, J. H., Schneider, N. M., Grogan, J. M. et al., Control of electron beam-induced Au nanocrystal growth kinetics through solution chemistry. Nano Lett., 15 (2015), 5314–5320.CrossRefGoogle ScholarPubMed
Mozumder, A., Fundamentals of Radiation Chemistry (London: Elsevier Science, 1999).Google Scholar
Mincher, B. J. and Wishart, J. F., The radiation chemistry of ionic liquids: a review. Solvent Extraction and Ion Exchange, 32 (2014), 563–583.CrossRefGoogle Scholar
Huang, J. Y., Zhong, L., Wang, C. M. et al., In situ observation of the electrochemical lithiation of a single SnO2 nanowire electrode. Science, 330 (2010), 1515–1520.CrossRefGoogle ScholarPubMed

Save book to Kindle

To save this book to your Kindle, first ensure no-reply@cambridge.org is added to your Approved Personal Document E-mail List under your Personal Document Settings on the Manage Your Content and Devices page of your Amazon account. Then enter the ‘name’ part of your Kindle email address below. Find out more about saving to your Kindle.

Note you can select to save to either the @free.kindle.com or @kindle.com variations. ‘@free.kindle.com’ emails are free but can only be saved to your device when it is connected to wi-fi. ‘@kindle.com’ emails can be delivered even when you are not connected to wi-fi, but note that service fees apply.

Find out more about the Kindle Personal Document Service.

Available formats
×

Save book to Dropbox

To save content items to your account, please confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your account. Find out more about saving content to Dropbox.

Available formats
×

Save book to Google Drive

To save content items to your account, please confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your account. Find out more about saving content to Google Drive.

Available formats
×